Fundamentals of Chemistry 1030
Measurements
WEAR SAFETY GLASSES

Laboratory Procedures

A. Determining Measurements and Data Collection

1. Measuring length: Use the meterstick to measure the length of the following items in centimeters (cm) using significant figures. Measure to the nearest 0.1 cm for all length masurements.

Your little fingernail _________ cm

The distance around your wrist _________ cm

The length of your shoe _________ cm

Your height _________ cm

2. Determine and record the length and width of the sides of the rectangle drawn on the board. Calculate the area of the rectangle using the formula: Area = L x W.

Compare your results to those of two other classmates.

Measurements     Length (cm)     Width (cm)         Area (cm2)

Person 1             ________         _________     __________

Person 2             ________         _________     __________

Person 3             ________         _________     __________
 

B. Comparing Metric and American Units of Length

1. Using a ruler and a meterstick, determine the number of centimeters (to 0.1 cm) that correspond to a distance of 12.0 inches.

12.0 inches = ______ cm

Divide the number of centimeters that you measured by 12.0 inches.  Be sure to show your calculations. The result is your experimental value for the number of centimeters in 1.0 inch.

Calculations:
 
 
 
 
 
 

Experimental conversion factor: __________cm/in
 
 

C. Measuring Volume of Solid

1. Volume of Solid Direct Measurement Obtain an unknown solid sample from your instructor.
a)  Record the unknown # ___________
b)  Record its shape. __________

c) Use the meterstick to determine the dimensions of the solid in centimeters. (Since the equation for determining volume depends on the shape of the object, use the chart below to determine which dimensions are needed to determine the volume of your solid object.  For example, if the object is a cube, only length is needed.)

length (L):________, width (W) :________, height (H) :________, diameter (D):_______

d) Use the table below to calculate the volume of the solid.

Shape                    Dimensions                                            Volume (cm3)

cube                         length (L)                                             V = L3

rectangular             length (L), width (W), height (H)             V = L x W x H

cylinder                 diameter (D), height (H)                          V = (3.14 x D2 x H)/4

Show formula and calculations:

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Calculated volume found by direct measurement: _____________.

2. Volume of a Solid by Volume Displacement When a solid object is submerged under water, it displaces the water by the amount of its own volume. The difference in the water level before and after the object is submerged is equal to the volume of the object submerged.

a) Obtain a 25-mL graduated cylinder and fill it with water until it is about half full. Record the volume of the water. Tie a piece of thread around your solid sample used in part C1 above, and slowly submerge it into the graduated cylinder being careful not to splash any drops of water on the sides of the cylinder. Record the new volume of the water to the nearest 0.1 mL.

Volume of water before object submerged: ________ mL

Volume of water after object submerged: ________ mL

Calculate the volume displaced by the object:
                    Vol after submerged - vol before submerged = vol displaced = vol of the solid in mL

b) Convert the volume of the solid from milliliters to cubic centimeters (1 mL = 1 cm3)
 
 
 
 

Calculated volume found by volume displacement: ___________ cm3
 

D. Determining the Mass of Solid

1. Demonstration: Your lab instructor will demonstrate the proper use of the laboratory balance.

Notes:
 
 
 
 
 
 
 
 

2. Mass of Solid: Determine the mass of your solid object using the balance (to the nearest 0.001g).

Mass of Solid: _________
 
 
 
 

E. Determining the Density of Solid

Density is defined as mass in grams per unit volume in milliliters or g/mL.

Density of solid = Mass (g) of solid/Volume (mL) of solid

1. Calculating the density of the solid: Using the mass of the solid that you determined in part D and the volume of the solid that you determined in part C (by displacement), calculate the density of your solid object.

Show your calculations:
 
 

Density of solid object: ______________

 

Questions to be addressed in your conclusion:

F What are some reasons that the resulting values for the area of the rectangle determined in part A might vary from person to person?

F In part B, how does your experimental conversion factor for cm to inches compare to the theoretical value of 2.54 cm/in?

F In part C, how close are the results for the volume of the solid from measuring the dimensions to the volume you determined
    by displacement of water?

F Which method of volume measurement do you think is most accurate: direct measurement or measurement by
     displacement ? Why?

F After having determined the density of a solid, briefly describe how you would propose to experimentally determine the
     density of a liquid.
 
  (updated 1-4-07  P Powers)